TY - JOUR
T1 - Evaluation of mechanical and thermal properties of commonly used denture base resins
AU - Phoenix, Rodney D.
AU - Mansueto, Michael A.
AU - Ackerman, Neal A.
AU - Jones, Robert E.
PY - 2004/3
Y1 - 2004/3
N2 - Purpose: The purpose of this investigation was to evaluate and compare the mechanical and thermal properties of 6 commonly used polymethyl methacrylate denture base resins. Materials and Methods: Sorption, solubility, color stability, adaptation, flexural stiffness, and hardness were assessed to determine compliance with ADA Specification No. 12. Thermal assessments were performed using differential scanning calorimetry and dynamic mechanical analysis. Results were assessed using statistical and observational analyses. Results: All materials satisfied ADA requirements for sorption, solubility, and color stability. Adaptation testing indicated that microwave-activated systems provided better adaptation to associated casts than conventional heat-activated resins. According to flexural testing results, microwaveable resins were relatively stiff, while rubber-modified resins were more flexible. Differential scanning calorimetry indicated that microwave-activated systems were more completely polymerized than conventional heat-activated materials. Conclusion: The microwaveable resins displayed better adaptation, greater stiffness, and greater surface hardness than other denture base resins included in this investigation. Elastomeric toughening agents yielded decreased stiffness, decreased surface hardness, and decreased glass transition temperatures.
AB - Purpose: The purpose of this investigation was to evaluate and compare the mechanical and thermal properties of 6 commonly used polymethyl methacrylate denture base resins. Materials and Methods: Sorption, solubility, color stability, adaptation, flexural stiffness, and hardness were assessed to determine compliance with ADA Specification No. 12. Thermal assessments were performed using differential scanning calorimetry and dynamic mechanical analysis. Results were assessed using statistical and observational analyses. Results: All materials satisfied ADA requirements for sorption, solubility, and color stability. Adaptation testing indicated that microwave-activated systems provided better adaptation to associated casts than conventional heat-activated resins. According to flexural testing results, microwaveable resins were relatively stiff, while rubber-modified resins were more flexible. Differential scanning calorimetry indicated that microwave-activated systems were more completely polymerized than conventional heat-activated materials. Conclusion: The microwaveable resins displayed better adaptation, greater stiffness, and greater surface hardness than other denture base resins included in this investigation. Elastomeric toughening agents yielded decreased stiffness, decreased surface hardness, and decreased glass transition temperatures.
KW - Adaptation
KW - Differential scanning calorimetry
KW - Dynamic mechanical analysis
KW - PMMA
KW - Thermal analysis
UR - http://www.scopus.com/inward/record.url?scp=2342466800&partnerID=8YFLogxK
U2 - 10.1111/j.1532-849X.2004.04002.x
DO - 10.1111/j.1532-849X.2004.04002.x
M3 - Article
C2 - 15032892
AN - SCOPUS:2342466800
SN - 1059-941X
VL - 13
SP - 17
EP - 27
JO - Journal of Prosthodontics
JF - Journal of Prosthodontics
IS - 1
ER -